Tert-Butylamine → N-(1,1-Dimethylethyl)benzenesulfonamide

Participants

Reaction Conditions

Reaction Steps

9.6 ml (75 mmol) of benzenesulphonic acid chloride are placed in 100 ml pyridine and 7.9 ml (75 mmol) of tert.butylamine are added dropwise at 5° C., whereupon the temperature increases to 35° C. After the addition has ended the mixture is stirred for another hour at 35° C. Then it is poured onto ice water and the crystalline precipitate is suction filtered.

Provenance & Evidence