HuagongsheHuagongshe Chemistry Print Report · For research reference only
Methanesulfonamide → HCID 10302452, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Methanesulfonamide | HCID 72879 | — |
| Reactant | HCID 22242280 | HCID 22242280 | — |
| Product | HCID 10302452 | HCID 10302452 | 67.6% |
Reaction Steps
3,5-Dibromo-4-(3-bromobenzyloxy)benzoic acid (0.15 mmol) was coupled with methanesulphonamide (0.77 mmol) using the procedure described in Example 31. Purification on column (silica gel, chloroform/methanol 9:1) gave 55 mg (67%) of N-[3,5-dibromo-4-(3-bromobenzyloxy)benzoyl]methanesulphonamide.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US07005538B1 |
| Source dataset | uspto-grants-2006_02 |
| ORD ID | ord-2b50343f36e0475596f24901e51f6c08 |
| Source note | uspto-grants-2006_02 |