反应详情

温度

100 °C

After the hydrolysis in the above step is complete, the reactor is cooled to about 100° C. and approximately 2.0 equivalents of sodium hydroxide (217 lbs of 50 weight percent solution), based upon the hydrochloric acid added in the production of 2-(decylthio)ethanamine hydrochloride, are introduced with stirring in approximately 30 minutes. The reaction mixture is allowed to settle until phase separation is complete (approximately 30 minutes) and the 2-(decylthio)ethanamine is decanted off. The 2-(decylthio)ethanamine can be passed over a drying agent such as sodium sulfate, or may be vacuum stripped to remove any dissolved and/or entrained water.

1. customAfter the hydrolysis in the above step
2. additionare introduced
3. customto settle until phase separation
4. custom(approximately 30 minutes)
5. customthe 2-(decylthio)ethanamine is decanted off
6. customto remove
7. dissolutionany dissolved