Styrene → HCID 18961255, compound

HRID 892397Notes

Reaction equation

HRID 892397 reaction equation
[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH3:9][C:10]([C:12]([O:14][CH2:15][CH2:16][OH:17])=[O:13])=[CH2:11]>C1COCC1>[CH2:1]=[CH:2][C:3]1[CH:8]=[CH:7][CH:6]=[CH:5][CH:4]=1.[CH3:11][C:10]([C:12]([O:14][CH2:15][CH2:16][OH:17])=[O:13])=[CH2:9]

Participants

4

Reactant 2

HCID 7501StyreneHCID 133602-Hydroxyethyl Methacrylate

Product 1

HCID 18961255HCID 18961255, compound

Reagents, catalysts & solvents 1

HCID 8028TetrahydrofuranSolvent

Procedure

The procedure of Example 5 was repeated. The charges of the components were as follows: CSHPU (125.0 g, 20% solids in THF), styrene (STY) (44.0 g), and HEMA (5.44 g). The solution was photolyzed for about 40 hours in order to obtain 80-85% conversion. DSC, GPC, OH equivalent weight, and other pertinent results obtained from the evaluation of the C$HPU/STY/HEMA copolymer obtained are given in Table I. The copolymer obtained was combined with CB-601 isocyanate curing agent and coated according to the procedure of Example 5. The percentage cure at room temperature was measured and set forth in Table I.

Workup

  1. customto obtain 80-85% conversion
  2. customDSC, GPC, OH equivalent weight, and other pertinent results

Sources & evidence

ORD record
ord-6ef52410dd1c4480a6037ccb19680715
Source dataset
uspto-grants-1992_06
Patent number
US05118580

Reaction notes

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