HuagongsheHuagongshe Chemistry Print Report · For research reference only
HCID 19895770, compound → HCID 19895762, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | HCID 19895770 | HCID 19895770 | — |
| Reactant | Aluminium lithium hydride | HCID 21226445 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19895762 | HCID 19895762 | — |
Reaction Steps
The product of Example 13 was reduced with LAH in dry THF and, after purification, the isolated compound was characterized by its HCl.salt NMR, (CD3OD) δ7.7 (m, 4H), 6.9 (m, 1H), 6.6 (m, 2H), 1.0 (t, 3H).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118704 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-76c1cb9457da4529824b74fee485dd75 |
| Source note | uspto-grants-1992_06 |