HuagongsheHuagongshe Chemistry Print Report · For research reference only
2,6-Diisopropylphenyl isocyanate → HCID 57081079, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2,6-Diisopropylphenyl isocyanate | HCID 92259 | — |
| Reactant | Lithium diisopropylamide | HCID 2724682 | — |
| Reactant | 2,3,4,5,6,7,8,9,10,11,12,13-Dodecahydro-1H-cyclopentacyclododecen-1-one | HCID 11031398 | — |
| Product | HCID 57081079 | HCID 57081079 | — |
Reaction Steps
The title compound, mp 225°-229° C., was prepared from bicyclo[10.3.0]pentadec-12(1)-en-13 one (5.0 g, 0.022 mol), 2,6-diisopropylphenyl isocyanate (4.60 g, 0.022 mol), and lithium diisopropylamide (0.022 mol) using the procedure described in Example 1. ##STR12##
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118697 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-ed50f3aa22844c6dab184f09ca5a34a5 |
| Source note | uspto-grants-1992_06 |