HuagongsheHuagongshe Chemistry Print Report · For research reference only
Ethyl Acetate → 2-(6-bromo-2,2-dimethyl-2H-1-benzopyran-4-yl)pyridine N-oxide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | 6-bromo-2,2-dimethyl-4-(2-pyridyl)-2H-1-benzopyran | HCID 19895587 | — |
| Product | 2-(6-bromo-2,2-dimethyl-2H-1-benzopyran-4-yl)pyridine N-oxide | HCID 53669139 | — |
Reaction Steps
In an analogous manner to that described in the first paragraph of Example 6, from 6-bromo-2,2-dimethyl-4-(2-pyridyl)-2H-1-benzopyran there was obtained 2-(6-bromo-2,2-dimethyl-2H-1-benzopyran-4-yl)pyridine N-oxide of melting point 146°-148° C. (from ethyl acetate).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05118694 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-e3a0fd2f092140009a9b8c0b747ecb34 |
| Source note | uspto-grants-1992_06 |