Hydrochloric Acid → HCID 19894083, compound

Participants

Reaction Steps

Hydrochloric acid in dioxanes (4M, 7 mL) was added to a solution of N-tert-butoxycarbonyl-N-methyl-3-aminobenzophenone (2.2 g, 7.4 mmol) in methylene chloride (5 mL). The mixture was stirred at room temperature for 1 hour and then concentrated. The residue was partitioned between chloroform and saturated sodium bicarbonate solution and the organic layer was washed with saturated sodium chloride and dried over sodium sulfate. The solvent was removed in vacuo to yield the desired product.

Provenance & Evidence