HuagongsheHuagongshe Chemistry Print Report · For research reference only
Thiazolidinedione → HCID 14459866, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Thiazolidinedione | HCID 5437 | — |
| Reactant | Ethyl Acetate | HCID 8857 | — |
| Reactant | HCID 14459965 | HCID 14459965 | — |
| Solvent | Hexane | HCID 8058 | — |
| Product | HCID 14459866 | HCID 14459866 | — |
Reaction Steps
By the method of Example 1, N-methyl-N-(2-phenylethyl)-4-(bromomethyl)benzenesulfonamide (10.6 mmol, 3.9 g) and thiazolidine-2,4-dione (11.7 mmol 1.4 g,), using 1:2 ethyl acetate:hexane as eluant, were converted to 3.3 g purified title product as a gum.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05120754 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-a82a6f9175c544fa9c886f87f00370c9 |
| Source note | uspto-grants-1992_06 |