P-Phenylenediamine → p-Oleoylaminoaniline

HRID 892878Notes

Reaction equation

[C:1]([OH:20])(=O)[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18].[CH:21]1[C:26]([NH2:27])=[CH:25][CH:24]=[C:23]([NH2:28])[CH:22]=1>>[C:1]([NH:27][C:26]1[CH:21]=[CH:22][C:23]([NH2:28])=[CH:24][CH:25]=1)(=[O:20])[CH2:2][CH2:3][CH2:4][CH2:5][CH2:6][CH2:7][CH2:8]/[CH:9]=[CH:10]\[CH2:11][CH2:12][CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH3:18]

Participants

Reactant 2

HCID 7814P-Phenylenediamine

HCID 445639Oleic Acid

Product 1

HCID 68840460p-OleoylaminoanilineYield 77%

Procedure

Oleic acid (2.82 g) and p-phenylenediamine (1.62 g) were reacted in the same manner as in Reference Example 11 to obtain 2.85 g of the objective compound (yield: 77%).

Sources & evidence

ORD record: ord-2a3f78e138014e389c96285c826b7455
Source dataset: uspto-grants-1992_06
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US05120738

Reaction notes

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