HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Iodide → Cyclohexyloxycarbonyloxymethyl iodide
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Iodide | HCID 5238 | — |
| Reactant | Chloromethyl cyclohexyl carbonate | HCID 13603586 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | Cyclohexyloxycarbonyloxymethyl iodide | HCID 11087296 | — |
Reaction Steps
A solution of 0.78 g of chloromethyl cyclohexyl carbonate and 1.0 g of sodium iodide in 15 ml of acetone is stirred at room temperature for 16 hours and then concentrated under reduced pressure. The residue is extracted with ether and the solvent is distilled off under reduced pressure to give the title compound as pale yellow oil.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05120841 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-f6f0345371204717bf40763b7b156307 |
| Source note | uspto-grants-1992_06 |