HRID892920

反应详情

EQUATION

反应方程式

HRID 892920 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

A solution of 0.78 g of chloromethyl cyclohexyl carbonate and 1.0 g of sodium iodide in 15 ml of acetone is stirred at room temperature for 16 hours and then concentrated under reduced pressure. The residue is extracted with ether and the solvent is distilled off under reduced pressure to give the title compound as pale yellow oil.

WORKUP

后处理

  1. concentrationconcentrated under reduced pressure
  2. extractionThe residue is extracted with ether
  3. distillationthe solvent is distilled off under reduced pressure