Hydrochloric Acid → HCID 131717427, compound

HRID 893011Notes

Reaction equation

HRID 893011 reaction equation
[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]1[N:8]=[N:9][C:10]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][N:21]=2)=[CH:11][C:12]=1[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][OH:19].[ClH:26]>O>[ClH:26].[ClH:26].[N:1]1[CH:6]=[CH:5][CH:4]=[CH:3][C:2]=1[C:7]1[N:8]=[N:9][C:10]([C:20]2[CH:25]=[CH:24][CH:23]=[CH:22][N:21]=2)=[CH:11][C:12]=1[CH2:13][CH2:14][CH2:15][CH2:16][CH2:17][CH2:18][OH:19]

Participants

4

Reactant 2

HCID 313Hydrochloric AcidHCID 70351602HCID 70351602, compound

Product 1

HCID 131717427HCID 131717427, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

3,6-Bis(2-pyridinyl)-4-pyridazine hexanol (EXAMPLE 17, 0.167 g) is dissolved in water (6 ml) containing hydrochoric acid (2 equivalents), filtered and freeze dried to give the title compound.

Workup

  1. filtrationfiltered
  2. customfreeze dried

Sources & evidence

ORD record
ord-cfd6b62a5b694a3c8ace653719d43f07
Source dataset
uspto-grants-1992_06
Patent number
US05120843

Reaction notes

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