HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrochloric Acid → HCID 19894619, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrochloric Acid | HCID 313 | — |
| Reactant | Diethyl Ether | HCID 3283 | — |
| Reactant | HCID 19894524 | HCID 19894524 | — |
| Solvent | Acetone diethylether | HCID 21584533 | — |
| Product | HCID 19894619 | HCID 19894619 | — |
Reaction Steps
2-[4-(4-(3,5-Dimethyl-4-methoxyphenyl)butyl)piperazin-1-yl]-N-ethyl-3-pyridineamine (EXAMPLE 43) is dissolved in ether/acetone and treated in excess with ether which was saturated with hydrogen chloride gas. The salt is filtered, dried under reduced pressure to give the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05120843 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-ef99f033f00f46dfba2a50732f4dbb84 |
| Source note | uspto-grants-1992_06 |