HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19096826, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Bromo-2-methylaniline | HCID 11423 | — |
| Reactant | Ethyl 1-(chlorocarbonyl)cyclopentane-1-carboxylate | HCID 19096799 | — |
| Solvent | Tetrahydrofuran | HCID 8028 | — |
| Product | HCID 19096826 | HCID 19096826 | 35% |
Reaction Steps
Ethyl 1-chlorocarbonylcyclopentanecarboxylate (3.10 grams, 0.02 mole) prepared in Example XX, 4-bromo-2-methylaniline (2.82 grams, 0.02 mole) and triethylamine (1.53 grams, 0.02 mole) were reacted in tetrahydrofuran (200 milliliters) under conditions similar to those described in Example I to give 2.40 grams (0.007 mole) of ethyl 1-(4-bromo-2-methylphenylaminocarbonyl)cyclopentanecarboxylate which, after recrystallization from hexane, had a melting point of 64° C.-67° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05123951 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-5c4b8dd403874011b3ee3510f3fea649 |
| Source note | uspto-grants-1992_06 |