HuagongsheHuagongshe Chemistry Print Report · For research reference only
Triethylamine → HCID 19096842, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Triethylamine | HCID 8471 | — |
| Reactant | 4-Bromo-2-methylaniline | HCID 11423 | — |
| Reactant | HCID 19096901 | HCID 19096901 | — |
| Product | HCID 19096842 | HCID 19096842 | 50% |
Reaction Steps
4-Bromo-2-methylaniline (2.83 grams, 0.01 mole), methyl chlorocarbonyl(dimethoxy)acetate (2.99 grams, 0.01 mole), prepared in Part A, and triethylamine (1.54 grams, 0.015 mole) were reacted in a manner similar to the procedure described in Example I to give 1.73 grams (0.005 mole) of methyl 3-[(4-bromo-2-methylphenyl)amino]-2,2-dimethoxy-3-oxopropanoate having a melting point of 99° C.-103° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05123951 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-6409dad00f444f61931132a6073ac710 |
| Source note | uspto-grants-1992_06 |