HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 19096838, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 3,5-Dichloroaniline | HCID 12281 | — |
| Reactant | HCID 85670801 | HCID 85670801 | — |
| Product | HCID 19096838 | HCID 19096838 | 28.6% |
Reaction Steps
Mono-n-propyl methoxymalonate (13.07 grams, 0.07 mole), prepared in Part B, 3,5-dichloroaniline (12.02 grams, 0.07 mole) and 1,3-dicyclohexylcarbodiimide (15.31 grams, 0.07 mole) were reacted in a manner similar to that described in Example LVII to give 7.22 grams (0.02 mole) of n-propyl 3-[(3,5-dichlorophenyl)amino]-2-methoxy-3-oxopropanoate having a melting point of 89° C.-93° C. An analytical sample recrystallized from hexane had a melting point of 89° C.-92° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05123951 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-ccc7c5488c45483caf0bd19096462525 |
| Source note | uspto-grants-1992_06 |