HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dicyclohexylcarbodiimide → HCID 19891458, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dicyclohexylcarbodiimide | HCID 10868 | — |
| Reactant | 4-Bromo-2-methylaniline | HCID 11423 | — |
| Reactant | HCID 19891463 | HCID 19891463 | — |
| Product | HCID 19891458 | HCID 19891458 | 46.7% |
Reaction Steps
Ethyl 2-carboxy-3-methyloxiranecarboxylate (5.09 grams, 0.03 mole), prepared in Part B, 4-bromo-2-methylaniline (5.44 grams, 0.03 mole) and 1,3-dicyclohexylcarbodiimide (6.03 grams, 0.03 mole) were reacted in a manner similar to that described in Example LVII to give 4.72 grams (0.014 mole) of N-(4-bromo-2-methylphenyl)-2-ethoxycarbonyl-3-methyloxiranecarboxamide having a melting point of 57° C.-60° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05123951 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-5e9fe3eeb0354d85b8face049f8d75b5 |
| Source note | uspto-grants-1992_06 |