HuagongsheHuagongshe Chemistry Print Report · For research reference only
m-Chloroperbenzoic acid → HCID 19782074, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | m-Chloroperbenzoic acid | HCID 70297 | — |
| Reactant | Calcium Hydroxide | HCID 6093208 | — |
| Reactant | HCID 19782078 | HCID 19782078 | — |
| Solvent | Chloroform | HCID 6212 | — |
| Product | HCID 19782074 | HCID 19782074 | — |
Reaction Steps
In 5 ml of chloroform was dissolved 340 mg of 7-(4-chlorobenzyl)-2,2-dimethyl-1-methylenecycloheptane [Compound (III-3) in Table III], and then 450 mg of m-chloroperbenzoic acid was added to the mixture over 10 minutes and the mixture was stirred at room temperature for one hour. Next, 385 mg of calcium hydroxide was added and the mixture was stirred at room temperature for 10 minutes.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05124345 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-dfa852c929c64b05a4fcdb062b5c8df9 |
| Source note | uspto-grants-1992_06 |