Ethyl bromoacetate → HCID 19890432, compound

Participants

Reaction Steps

In a nitrogen atmosphere, 31.47 g (120 mM) of triphenylphosphine was added to 60 ml of benzene, and 23.38 g (140 mM) of ethyl bromoacetate was added under cooling with ice. After 1 hour of stirring at room temperature, the resultant precipitate salt was taken out by filtration and washed with benzene to obtain 48.90 g of ethyl acetate-triphenyl phosphonium bromide. Yield: 95%.

Provenance & Evidence