Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Pyridine | HCID 1049 | — |
| Reactant | 2-Chloroacetophenone | HCID 10757 | — |
| Solvent | Acetonitrile | HCID 6342 | — |
| Product | HCID 12266211 | HCID 12266211 | — |
Reaction Steps
Phenacylpyridinium chloride was prepared by reacting 424 grams chloroacetophenone with 322 ml pyridine by dropwise adding the pyridine to the former in 1400 ml acetonitrile at 65° C. A crystalline mass was obtained which was heated to 70° C. and allowed to cool to 10° C., then filtered and washed with 500 ml acetonitrile. The dried product (626.5g) had a melting point of 203-206° C.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US05126233 |
|---|
| Source dataset | uspto-grants-1992_06 |
|---|
| ORD ID | ord-ece249515f6942958d0801be21b7a199 |
|---|
| Source note | uspto-grants-1992_06 |
|---|
