HuagongsheHuagongshe Chemistry Print Report · For research reference only
Sodium Hydroxide → HCID 19890936, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Sodium Hydroxide | HCID 14798 | — |
| Reactant | HCID 19890935 | HCID 19890935 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 19890936 | HCID 19890936 | — |
Reaction Steps
A solution of 0.5 g (0.00113 mol) 2-(2-picolylseleno)-N-(4-pyridyl)benzamide dihydrochloride from Example 5 in 2 ml H2O is made alkaline with 10 N NaOH and extracted twice with 5 ml portions of dichloromethane. The organic phase is dried over magnesium sulfate, the solvent removed and the crude product recrystallized from 15 ml 2-propanol.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05126357 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-ac47ec2cefd94c52bec09dd3c1b2d0b8 |
| Source note | uspto-grants-1992_06 |