Hydroxyamine hydrochloride → HCID 73656502, compound

Participants

Reaction Steps

5.6 g of the α-(2-thienyl)aminoacetonitrile thus obtained was dissolved in 30 ml of methanol and 2.8 g of hydroxylamine hydrochloride was added thereto in a water bath. After stirring for a while, the mixture began to crystallize while showing slight heat generation. The mixture was stirred at room temperature for several hours thereafter. After the completion of the reaction, the reaction mixture was concentrated and the solvent was distilled off. After recrystallizing from ethanol, 7.6 g of the aimed α-(2-thienyl)aminoacetamidoxime hydrochloride was obtained.

Provenance & Evidence