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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 893756Generated: October 29, 2026

Trifluoroacetic acid → HCID 131717438, compound

https://huagongshe.com/reaction/893756

Reaction equation

Participants

RoleNameHCIDCharge
ReactantTrifluoroacetic acidHCID 6422—
ReactantHCID 131717440HCID 131717440—
SolventDiisopropyl EtherHCID 7914—
ProductHCID 131717438HCID 131717438—

Reaction Steps

Diphenylmethyl 7-t-butoxycarbonylamino-3-[(E)-3-(5,6-diacetoxy-2-methyl-2-isoindolinio)-1-propen-1-yl]-3-cephem-4-carboxylate iodide (Va) (610 mg, 0.69 mmol) was treated with TFA (6 ml) at room temperature for 30 min. The reaction mixture was diluted with isopropyl ether. The resulting precipitate was collected by filtration to yield 502 mg (quantitative yield) of the title compound.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS05126336
Source datasetuspto-grants-1992_06
ORD IDord-5942ceb183e44d2aaedab5f8ac49fb5e
Source noteuspto-grants-1992_06