HuagongsheHuagongshe Chemistry Print Report · For research reference only
Trifluoroacetic acid → HCID 131717438, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Trifluoroacetic acid | HCID 6422 | — |
| Reactant | HCID 131717440 | HCID 131717440 | — |
| Solvent | Diisopropyl Ether | HCID 7914 | — |
| Product | HCID 131717438 | HCID 131717438 | — |
Reaction Steps
Diphenylmethyl 7-t-butoxycarbonylamino-3-[(E)-3-(5,6-diacetoxy-2-methyl-2-isoindolinio)-1-propen-1-yl]-3-cephem-4-carboxylate iodide (Va) (610 mg, 0.69 mmol) was treated with TFA (6 ml) at room temperature for 30 min. The reaction mixture was diluted with isopropyl ether. The resulting precipitate was collected by filtration to yield 502 mg (quantitative yield) of the title compound.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US05126336 |
| Source dataset | uspto-grants-1992_06 |
| ORD ID | ord-5942ceb183e44d2aaedab5f8ac49fb5e |
| Source note | uspto-grants-1992_06 |