Methanol → HCID 53843919, compound

Participants

Reaction Steps

To 0.5 ml of methanol was added 0.17 g of (R)-(-)-2-fluoro-2-(trifluoromethyl)hexanoyl chloride, and this mixture was stirred at room temperature for 30 minutes. The resulting reaction mixture was distilled with Kugelrohr under atomspheric pressure, thereby obtaining 0.15 g of methyl (S)-(-)-2-fluoro-2-(trifluoromethyl)hexanoate having the physical properties as mentioned hereinbefore.

Provenance & Evidence