HuagongsheHuagongshe Chemistry Print Report · For research reference only
Salicylic acid, hydrazide → HCID 178513059, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Salicylic acid, hydrazide | HCID 13637 | — |
| Reactant | Methyl 2,2,2-trichloroacetimidate | HCID 100479 | — |
| Product | HCID 178513059 | HCID 178513059 | 100% |
Reaction Steps
A mixture of 3.8 g (0.025 mole) salicoylhydrazine and 10 ml (14.3 g, 0.08 mole) methyl 2,2,2-trichloroacetimidate was stirred 16 hours at room temperature. The solid that formed was washed with petroleum ether and dried to give 7.5 g (100% Yield; mp 168°-169° C.). The structure was confirmed via infrared and elemental analysis.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04282169 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-88e76842bc034e489c23448c2f0c5573 |
| Source note | uspto-grants-1981_08 |