Dimethyl N-cyanodithioiminocarbonate → HCID 136100175, compound

HRID 894135Notes

Reaction equation

HRID 894135 reaction equation
[Cl:1][C:2]1[C:3]([CH2:8][S:9][CH2:10][CH2:11][CH2:12][NH2:13])=[N:4][CH:5]=[CH:6][CH:7]=1.[C:14]([N:16]=[C:17](SC)SC)#[N:15].[CH2:22]([NH2:25])[C:23]#[CH:24]>>[C:14]([NH:16][C:17]([NH:25][CH2:22][C:23]#[CH:24])=[N:13][CH2:12][CH2:11][CH2:10][S:9][CH2:8][C:3]1[C:2]([Cl:1])=[CH:7][CH:6]=[CH:5][N:4]=1)#[N:15]

Participants

4

Reactant 3

HCID 66289Dimethyl N-cyanodithioiminocarbonateHCID 239041PropargylamineHCID 20570288HCID 20570288, compound

Product 1

HCID 136100175HCID 136100175, compound

Procedure

Reaction of 3-[(3-chloro-2-pyridyl)methylthio]propylamine with dimethyl cyanodithioimidocarbonate and treatment of the resultant product with propargylamine according to the general procedure of Example 4 gives the title compound.

Sources & evidence

ORD record
ord-8cdb669ccf554952b9dc2a4cf2adae03
Source dataset
uspto-grants-1981_08
Patent number
US04282363

Reaction notes

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