Hydrochloric Acid → HCID 12929145, compound

HRID 894203Notes

Reaction equation

HRID 894203 reaction equation
[CH3:1][S:2]([CH:5]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[CH2:9][O:8][C:7]2[CH:16]=[CH:17][C:18]([C:20]([O:22]C)=[O:21])=[CH:19][C:6]1=2)(=[O:4])=[O:3].[OH-].[Na+].Cl>O>[CH3:1][S:2]([CH:5]1[C:11]2[CH:12]=[CH:13][CH:14]=[CH:15][C:10]=2[CH2:9][O:8][C:7]2[CH:16]=[CH:17][C:18]([C:20]([OH:22])=[O:21])=[CH:19][C:6]1=2)(=[O:4])=[O:3]

Participants

5

Reactant 3

HCID 313Hydrochloric AcidHCID 14798Sodium HydroxideHCID 21162713HCID 21162713, compound

Product 1

HCID 12929145HCID 12929145, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

Reflux 1 gm. of the ester of Step A and 40 cc. of 1 N aqueous sodium hydroxide for 15 minutes. Strip to dryness and dissolve the residue in water. Acidify with aqueous hydrochloric acid. Separate the solids by filtration to obtain the title product (m.p. 251° C. dec.).

Workup

  1. temperatureReflux 1 gm
  2. customSeparate the solids
  3. filtrationby filtration

Sources & evidence

ORD record
ord-f95130f624694dc18cad3d9e7606e10a
Source dataset
uspto-grants-1981_08
Patent number
US04282365

Reaction notes

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