Hydrogen Peroxide → HCID 21162717, compound

Participants

Reaction Conditions

Reaction Steps

Dissolve with warming 380 mg. of 6,11-dihydro-11-methylthiodibenz[b,e]oxepin-2-carboxylic acid in 38 ml. of glacial acetic acid. Place the reaction mixture in an oil bath at 40° C. and add 1.5 ml. of 30% hydrogen peroxide. Stir the mixture at 40° C. for 3 1/2 hours until the solution clears. Dilute with 300 ml. of water and separate the precipitate by filtration to obtain the title product.

Provenance & Evidence