Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Formamide | HCID 713 | — |
| Reactant | HCID 10446851 | HCID 10446851 | — |
| Solvent | Water | HCID 962 | — |
| Product | HCID 21162715 | HCID 21162715 | 90% |
Reaction Steps
Add 2.35 gm. of methyl 6,11-dihydro-11-chlorodibenz[b,e]oxepin-2-carboxylate to 20 ml. of formamide. Stir and heat the mixture at 110° C. for 3 hours. Cool to room temperature, dilute with water and separate the solids by filtration to obtain the title product (Yield 2.18 gm., 90%).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US04282365 |
|---|
| Source dataset | uspto-grants-1981_08 |
|---|
| ORD ID | ord-68785163ecec4292942d528e6d61d2e1 |
|---|
| Source note | uspto-grants-1981_08 |
|---|
