Potassium Hydroxide → HCID 23720707, compound

HRID 894255Notes

Reaction equation

HRID 894255 reaction equation
[Cl:1][C:2]1[CH:3]=[C:4]([S:8][C:9]2[O:13][CH:12]=[C:11]([C:14]([O-:16])=[O:15])[CH:10]=2)[CH:5]=[CH:6][CH:7]=1.[OH-].[K+:18]>C(OCC)(=O)C>[Cl:1][C:2]1[CH:3]=[C:4]([S:8][C:9]2[O:13][CH:12]=[C:11]([C:14]([O-:16])=[O:15])[CH:10]=2)[CH:5]=[CH:6][CH:7]=1.[K+:18]

Participants

4

Reactant 2

HCID 14797Potassium HydroxideHCID 21162466HCID 21162466, compound

Product 1

HCID 23720707HCID 23720707, compound

Reagents, catalysts & solvents 1

HCID 8857Ethyl AcetateSolvent

Procedure

5-(3-Chlorophenylthio)furan-3-carboxylate is dissolved in ethyl acetate. An equivalent of ethanolic potassium hydroxide is added. Potassium 5-(3-chlorophenylthio)furan-3-carboxylate is isolated by concentration to dryness or by precipitation resulting from addition of a non-solvent (ether or heptane).

Sources & evidence

ORD record
ord-6aedd073c05b49b99eb7a415d93c5e9f
Source dataset
uspto-grants-1981_08
Patent number
US04282246

Reaction notes

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