2-Bromo-1,2-diphenylethan-1-one → HCID 20575031, compound

Participants

Reaction Steps

A 2.16 g. portion of hexahydro-1,3-diazocine-2(1H)-thione is dissolved in 800 ml. of hot acetone. The solution is clarified and then stirred as 4.2 g. of 2-bromo-2-phenylacetophenone in 50 ml. of acetone is added. The solution is stirred at room temperature for 7 hours, then the solid is collected, washed with 200 ml. of acetone and dried in vacuo at 60° C., giving 5.1 g. of the desired product, m.p. 211°-213° C. (dec.).

Provenance & Evidence