HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-Bromopropiophenone → HCID 20575036, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-Bromopropiophenone | HCID 16452 | — |
| Reactant | 1,3-Diazocane-2-thione | HCID 5372734 | — |
| Solvent | Acetone | HCID 180 | — |
| Product | HCID 20575036 | HCID 20575036 | — |
Reaction Steps
A mixture of 1.44 g. of hexahydro-1,3-diazocine-2(1H)-thione and 500 ml. of acetone is heated to produce solution. A 2.13 g. portion of 2-bromopropiophenone is added and the mixture is allowed to stand overnight. The solid is collected, washed with acetone and dried, giving 2.53 g. of the desired product, m.p. 191°-193° C. (dec.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04283334 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-c3640c80029f48e6aec9d66022422c86 |
| Source note | uspto-grants-1981_08 |