HuagongsheHuagongshe Chemistry Print Report · For research reference only
Diethyl Succinate → HCID 20532902, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Diethyl Succinate | HCID 31249 | — |
| Reactant | 2,4-Dimethylphenylacetonitrile | HCID 144303 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 20532902 | HCID 20532902 | 78% |
Reaction Steps
This material was prepared using 130.65 g (0.750 mol) of diethyl succinate, 72.60 g (0.500 mol of 2,4-dimethylbenzyl cyanide, 14.95 g (0.65 mol) of sodium, and 168 ml of dry ethanol using the procedure described in Part A of Example I. The product was obtained as a dark red oil, 106.5 g (78% yield).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04283348 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-16fea77b96534d6fa4e6d733ef0c69b3 |
| Source note | uspto-grants-1981_08 |