HuagongsheHuagongshe Chemistry Print Report · For research reference only
Hydrazine → HCID 12889662, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Hydrazine | HCID 9321 | — |
| Reactant | HCID 12889638 | HCID 12889638 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | HCID 12889662 | HCID 12889662 | — |
Reaction Steps
A 25 g. portion of the product of Example 1 was reacted with excess hydrazine in 200 ml. of ethanol for 2 hours, allowing the reaction to heat to reflux temperature. The solids which precipitated upon cooling were separated by filtration and identified as 27 g. of product, m.p. 115°-117°, NMR singlets at 4.48, 7.4, 7.63, 7.97 and 8.73 ppm., and multiplets at 3.05-4.12 and 4.67-5.28 ppm.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04283403 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-b566dea1a1514aaca11ce9b713a2511d |
| Source note | uspto-grants-1981_08 |