HRID894368

反应详情

EQUATION

反应方程式

HRID 894368 的结构方程式

AUXILIARIES

试剂、催化剂与溶剂

1

PROCEDURE

实验过程

BuOK in 300 cm3 of anhydrous dimethylsulfoxide and 15.5 g of ethyl 1-tert-butyl-cyclohexyl-carboxylate were heated for 7 hours at 110° C. The mixture was then poured on ice. By acidification with dilute HCl the tert-butyl-cyclohexyl-carboxylic acid was precipitated.

WORKUP

后处理

  1. additionThe mixture was then poured on ice
  2. customBy acidification with dilute HCl the tert-butyl-cyclohexyl-carboxylic acid was precipitated