HuagongsheHuagongshe Chemistry Print Report · For research reference only
Potassium Carbonate → HCID 3837308, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Potassium Carbonate | HCID 11430 | — |
| Reactant | 2,6-Dichloroaniline | HCID 11846 | — |
| Reactant | HCID 10925153 | HCID 10925153 | — |
| Catalyst | Copper | HCID 23978 | — |
| Solvent | O-Xylene | HCID 7237 | — |
| Product | HCID 3837308 | HCID 3837308 | 81.8% |
Reaction Steps
A mixture of 6.0 g (0.019 mole) of N,N-diethyl(o-iodophenyl)acetamide, 3.38 g (0.021 mole) of 2,6-dichloroaniline, 2.93 g (0.021 mole) of anhydrous potassium carbonate, 1.0 g of copper powder and 1.0 g of cuprous iodide was reacted in 85 ml of xylene for 24 hours to obtain 5.46 g of a colorless needle having a melting point of 99° to 101° C. The yield was 81.4%.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04283532 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-d17d6d2c6fab4080a449a03a08cf7573 |
| Source note | uspto-grants-1981_08 |