Water → HCID 12926286, compound

Participants

Reaction Steps

10 g of N-(1'-phenoxy-2',2',2'-trichloroethyl)-2-hydroxybenzamide and 1.8 g of methyl isocyanate were dissolved in 150 mml of acetone. Two or three drops of triethylamine were added to the solution under stirring. After allowing to stand overnight, the reaction mixture was poured into water and the crystals which thus resulted were recrystallized from methanol to obtain 4.2 g of N-(1'-phenoxy-2',2',2'-trichloroethyl)-2-methylcarbamoyloxybenzamide as white crystals. Melting point: 138°-141° C.

Provenance & Evidence