HuagongsheHuagongshe Chemistry Print Report · For research reference only
Imidazole → 1-Cyclooctylmethylimidazole
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Imidazole | HCID 795 | — |
| Reactant | Sodium | HCID 5360545 | — |
| Reactant | Cyclooctane methyl bromide | HCID 20574510 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | 1-Cyclooctylmethylimidazole | HCID 20550238 | — |
Reaction Steps
Cyclooctane methyl bromide (5.5 g, 0.027 mole) was added dropwise to a refluxing solution of imidazole (2.0 g, 0.03 mole) in a solution of sodium (0.7 g, 0.03 mole) in absolute ethanol (50 ml). After addition the mixture was refluxed for a further 15 hours.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04284641 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-86565ee5294d480d8d58018a4e38c497 |
| Source note | uspto-grants-1981_08 |