HuagongsheHuagongshe Chemistry Print Report · For research reference only
O-((2-methylthiazol-4-yl)methyl)hydroxylamine → HCID 53718792, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | O-((2-methylthiazol-4-yl)methyl)hydroxylamine | HCID 425143 | — |
| Reactant | (2-Formamido-1,3-thiazol-4-yl)(oxo)acetic acid | HCID 13116693 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | HCID 53718792 | HCID 53718792 | 65.2% |
Reaction Steps
A mixture of 2-(2-formamidothiazol-4-yl)glyoxylic acid (1.10 g.) and 2-methylthiazol-4-ylmethoxyamine (0.99 g.) in methanol (17 ml.) was stirred at room temperature for 3 hours. The precipitates were collected by filtration and washed with methanol to give 2-(2-formamidothiazol-4-yl)-2-(2-methylthiazol-4-ylmethoxyimino)-acetic acid (syn isomer, 1.17 g.).
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04284631 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-42bdba8debd3498097020434757c8e68 |
| Source note | uspto-grants-1981_08 |