HuagongsheHuagongshe Chemistry Print Report · For research reference only
Dimethyl Sulfate → HCID 20572385, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Dimethyl Sulfate | HCID 6497 | — |
| Reactant | Sodium Bicarbonate | HCID 516892 | — |
| Reactant | HCID 20572383 | HCID 20572383 | — |
| Product | HCID 20572385 | HCID 20572385 | — |
Reaction Steps
The same method as in Example 2 is carried out using 56.7 parts of N-(2,2,2-trifluoroethyl)-m-toluidine, 53 parts of sodium bicarbonate and 75 parts of dimethyl sulphate. 52.8 parts, i.e. a yield equal to 86.7% of the theoretical yield, of N-methyl N-(2,2,2-trifluoroethyl)-m-toluidine are obtained.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US04285696 |
| Source dataset | uspto-grants-1981_08 |
| ORD ID | ord-663f9ac7afe34269afccae55159f719e |
| Source note | uspto-grants-1981_08 |