HRID894965

反应详情

EQUATION

反应方程式

HRID 894965 的结构方程式

PROCEDURE

实验过程

A mixture of 200 g. (0.826 mole) of 3-benzyloxybenzene-2-propanol in 50 ml. of hexane and 1 l. of concentrated hydrochloric acid is shaken for 15 minutes in a 2 l. separatory funnel. The organic layer is removed and washed with saturated sodium bicarbonate. The neutralized organic extent is dried over magnesium sulfate and evaporated to give a quantitative yield of the title compound as an oil.

WORKUP

后处理

  1. additionA mixture of 200 g
  2. customThe organic layer is removed
  3. washwashed with saturated sodium bicarbonate
  4. dry with materialThe neutralized organic extent is dried over magnesium sulfate
  5. customevaporated