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HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 894992Generated: October 25, 2026

2-(Diisopropylamino)ethyl chloride → 1-(Diisopropylamino-ethoxyimino)cyclododecane

https://huagongshe.com/reaction/894992

Reaction equation

Participants

RoleNameHCIDCharge
Reactant2-(Diisopropylamino)ethyl chlorideHCID 7312—
ReactantSodium hydrideHCID 24758—
ReactantCyclododecanone, oximeHCID 136762—
ReactantFumarate(1-)HCID 6183479—
Product1-(Diisopropylamino-ethoxyimino)cyclododecaneHCID 13205805—

Reaction Steps

Starting from 2.4 g. (0.1 moles) of sodium hydride, 19.73 g. (0.1 moles) of cyclododecanone oxime and 17.95 g. (0.11 moles) of 1-diisopropylamino-2-chloroethane the title compound is prepared as in Example 1. Yield: 22.1 g. (68.20%); b.p.: 164°-166° C./0.6 torr. Hydrogen fumarate, m.p.: 120°-121° C.

Provenance & Evidence

DOI10.6084/m9.figshare.5104873.v1
Patent numberUS04285942
Source datasetuspto-grants-1981_08
ORD IDord-f9fcca4175f547d8959ec27e0912e2f1
Source noteuspto-grants-1981_08