HuagongsheHuagongshe Chemistry Print Report · For research reference only
Boron tribromide → 1-Fluoro-6-(4-hydroxy-phenyl)-naphthalen-2-ol
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | Boron tribromide | HCID 25134 | — |
| Reactant | 2-Methoxy-6-(4-methoxyphenyl)-1-fluoronaphthalene | HCID 11219781 | — |
| Product | 1-Fluoro-6-(4-hydroxy-phenyl)-naphthalen-2-ol | HCID 10214633 | — |
Reaction Steps
The title compound was prepared by reacting 2-methoxy-6-(4-methoxyphenyl)-1-fluoronaphthalene (0.250 g, 0.886 mmol) with boron tribromide (2.7 mL of 1 N solution, 2.7 mmol) according to method D to yield 0.13 g (15%) of a white solid: mp 219-224° C.;
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06914074B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-0b43989b4c1648188693b3144c842858 |
| Source note | uspto-grants-2005_07 |