2-Bromonaphthalene → HCID 22048151, compound

Participants

Reaction Steps

The title compound was prepared by reacting 2-bromonaphthalene (0.31 g, 1.50 mmol) with 3-fluoro-4-methoxyphenylboronic acid (0.31 g, 1.80 mmol) according to method A to yield 0.30 g (79%) of a white solid: mp 108-110° C.; 1H NMR (CDCl3): δ (3.96, 3H, s), 7.04-7.10 (1H, m), 7.43-7.52 (4H, m), 7.68 (1H, dd, J=1.81 Hz, J=8.57 Hz), 7.84-7.92 (3H, m), 7.97 (1H, d, J=1.05 Hz).

Provenance & Evidence