Methyl Acrylate → HCID 15828539, compound

HRID 895315Notes

Reaction equation

[C:1]([O:5][CH3:6])(=[O:4])[CH:2]=[CH2:3].[CH2:7]([NH2:11])[CH2:8][CH2:9][CH3:10]>>[CH2:7]([N:11]([CH2:3][CH2:2][C:1]([O:5][CH3:6])=[O:4])[CH2:3][CH2:2][C:1]([O:5][CH3:6])=[O:4])[CH2:8][CH2:9][CH3:10]

Participants

Reactant 2

HCID 7294Methyl Acrylate

HCID 8007Butylamine

Product 1

HCID 15828539HCID 15828539, compoundYield 99.6%

Procedure

At 20 to 30° C., 12.9 g of methyl acrylate was added to 5.00 g of n-butylamine. The resulting mixture was allowed to stand for 20 hours, followed by concentration under reduced pressure, whereby 16.7 g of N-butylbis[2-(methoxycarbonyl)ethyl]amine was obtained (at a quantitative yield).

Workup

concentrationfollowed by concentration under reduced pressure

Sources & evidence

ORD record: ord-1e9f13e4cc1f42518de0015d1608fbc9
Source dataset: uspto-grants-2005_07
DOI: 10.6084/m9.figshare.5104873.v1
Patent number: US06916593B2

Reaction notes

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