HuagongsheHuagongshe Chemistry Print Report · For research reference only
HRID 895610Generated: November 1, 2026
Ammonium formate → 2-(4-Diethylcarbamoylbenzyl)anisole
https://huagongshe.com/reaction/895610
Participants
| Role | Name | HCID | Charge |
|---|
| Reactant | Ammonium formate | HCID 2723923 | — |
| Reactant | 1-(4-Diethylcarbamoylphenyl)-1-(2-methoxyphenyl)methyl acetate | HCID 69718877 | — |
| Catalyst | Palladium | HCID 23938 | — |
| Solvent | Methanol | HCID 887 | — |
| Product | 2-(4-Diethylcarbamoylbenzyl)anisole | HCID 22380682 | — |
Reaction Steps
The obtained 1-(4-diethylcarbamoylphenyl)-1-(2-methoxyphenyl)methyl acetate was dissolved in methanol (280 ml), added with 10% palladium/carbon (7 g) and ammonium formate (28.44 g) under argon atmosphere and stirred at 60° C. for 2 hours. After insoluble matters were removed by filtration, the solvent was evaporated under reduced pressure to obtain 2-(4-diethylcarbamoylbenzyl)anisole.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|
| Patent number | US06916822B2 |
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| Source dataset | uspto-grants-2005_07 |
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| ORD ID | ord-ecde1a821f8141839824f1327d1885dc |
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| Source note | uspto-grants-2005_07 |
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