HuagongsheHuagongshe Chemistry Print Report · For research reference only
2-(2-Methyl-2-nitropropyl)naphthalene → alpha,alpha-Dimethyl-2-naphthaleneethanamine
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 2-(2-Methyl-2-nitropropyl)naphthalene | HCID 9964618 | — |
| Catalyst | Nickel | HCID 935 | — |
| Solvent | Ethanol | HCID 702 | — |
| Product | alpha,alpha-Dimethyl-2-naphthaleneethanamine | HCID 15369616 | — |
Reaction Steps
Raney nickel W2 (200 mg) was suspended in ethanol (10 ml), to the suspension was added 2-(2-methyl-2-nitropropyl)naphthalene (134 mg) obtained in Step 5, and hydrogenation was performed at a pressure of 3.5 atom for 12 hr.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06916956B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-850220ed51ca439d8c25e5a01a31a0ff |
| Source note | uspto-grants-2005_07 |