Phthalazine → HCID 86759350, compound

HRID 895967Notes

Reaction equation

HRID 895967 reaction equation
[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[N:3][N:2]=1.[N+]([O-])([O-])=O.[Ag+:15]>O>[Ag:15].[CH:1]1[C:10]2[C:5](=[CH:6][CH:7]=[CH:8][CH:9]=2)[CH:4]=[N:3][N:2]=1

Participants

4

Reactant 2

HCID 9207PhthalazineHCID 24470Silver Nitrate

Product 1

HCID 86759350HCID 86759350, compound

Reagents, catalysts & solvents 1

HCID 962WaterSolvent

Procedure

A silver-phthalazine dispersion (1:1 molar ratio) was prepared by first dissolving 1.96 g phthalazine and 0.78 g of 35% gelatin solution (cattle bone, alkali treated, deionized gelatin) in 37.2 g demineralized water. This solution was stirred vigorously at room temperature while adding 4.70 g of 5.72 M AgNO3 solution.

Sources & evidence

ORD record
ord-72c584f43b5b4e8c8c303829f2b5124e
Source dataset
uspto-grants-2005_07
Patent number
US06919171B2

Reaction notes

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