HuagongsheHuagongshe Chemistry Print Report · For research reference only
5-Bromo-2-furanecarboxylic acid → HCID 9943685, compound
Participants
| Role | Name | HCID | Charge |
|---|---|---|---|
| Reactant | 5-Bromo-2-furanecarboxylic acid | HCID 68511 | — |
| Reactant | Bromotrimethylsilane | HCID 76113 | — |
| Reactant | Diethyl (aminomethyl)phosphonate | HCID 1596920 | — |
| Product | HCID 9943685 | HCID 9943685 | — |
Reaction Steps
5-Bromofuroic acid was reacted with diethyl aminomethylphosphonate in a manner similar to that described in Step D, Example 5. The product was treated with TMSBr as described in Step D, Example 1 to provide the title compound (no. 8.01) as a solid. HPLC Rt=3.72 min; negative ion electrospray MS M−1 found: 282/284.
Provenance & Evidence
| DOI | 10.6084/m9.figshare.5104873.v1 |
|---|---|
| Patent number | US06919322B2 |
| Source dataset | uspto-grants-2005_07 |
| ORD ID | ord-700535a5e5684ba289472c5d1478e5cb |
| Source note | uspto-grants-2005_07 |